2-Methoxyethylamine → N-(2-methoxyethyl)methanesulfonamide
反応式
[CH3:1][O:2][CH2:3][CH2:4][NH2:5].C(N(CC)CC)C.[CH3:13][S:14](Cl)(=[O:16])=[O:15]>ClCCl>[CH3:1][O:2][CH2:3][CH2:4][NH:5][S:14]([CH3:13])(=[O:16])=[O:15]参加物
5
実験手順
To a stirring solution of 2-methoxyethylamine (0.58 ml) in dichloromethane (10 ml) was added triethylamine (1.0 ml) and methanesulphonyl chloride (0.51 ml). The mixture was stirred at room temperature overnight. The solvents were removed in vacuo to give a crude product which was purified by flash chromatography to give N-(2-Methoxy-ethyl)-methanesulfonamide (0.74 g).
後処理
- customThe solvents were removed in vacuo
- customto give a crude product which
- customwas purified by flash chromatography
出典と根拠
- ORDレコード
- ord-5c533c63910049a7973a3ff144baf9cf
- 出典データセット
- uspto-grants-2013_05
- 特許番号
- US08450315B2
反応ノート
読み込み中…