Sodium Hydroxide → HCID 86613671、化合物

HRID 2105632ノート

反応式

HRID 2105632 の反応式
[CH2:1]([C@H:7]1[CH2:11][CH:10]([CH3:12])[O:9][C:8]1=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[OH-:14].[Na+:15]>C(O)C>[OH:9][CH:10]([CH3:12])[CH2:11][C@H:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[C:8]([O-:13])=[O:14].[Na+:15]

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 57809406(3S)-3-Hexyl-5-methyloxolan-2-one

生成物 1

HCID 86613671HCID 86613671、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

反応条件

温度
75 °C

実験手順

To an ethanol solution of the compound prepared in Example 1(6) was added an equivalent of an aqueous solution of sodium hydroxide, and the mixture was stirred at 75° C. for 3 hours. The reaction mixture was concentrated to give the compound of the present invention having the following physical data.

後処理

  1. concentrationThe reaction mixture was concentrated
  2. customto give the compound of the present invention

出典と根拠

ORDレコード
ord-1516e44be0fa4d68829fa8e60baec042
出典データセット
uspto-grants-2009_08
特許番号
US07579375B2

反応ノート

読み込み中…