5-(2-Chloroacetyl)-1,3-dihydro-3-methyl-2H-indol-2-one → HCID 15111515、化合物
反応式
Cl[CH2:2][C:3]([C:5]1[CH:6]=[C:7]2[C:11](=[CH:12][CH:13]=1)[NH:10][C:9](=[O:14])[CH:8]2[CH3:15])=O.[C:16]([O:20]C)(=[S:19])[NH:17][NH2:18]>C(#N)C>[O:20]=[C:16]1[NH:17][N:18]=[C:3]([C:5]2[CH:6]=[C:7]3[C:11](=[CH:12][CH:13]=2)[NH:10][C:9](=[O:14])[CH:8]3[CH3:15])[CH2:2][S:19]1参加物
4
実験手順
1.0 g 5-(2-chloroacetyl)-1,3-dihydro-3-methyl-2H-indol-2-one, 0.37 g O-methyl thiocarbazate, and 20 ml acetonitrile were refluxed for 2 hrs. The precipitate was isolated by filtration and washed with hot acetonitrile to yield a yellowish powder, 450 mg.
後処理
- customThe precipitate was isolated by filtration
- washwashed with hot acetonitrile
- customto yield a yellowish powder, 450 mg
出典と根拠
- ORDレコード
- ord-3e043bc9bf1745018843c558e1c8407d
- 出典データセット
- uspto-grants-1990_06
- 特許番号
- US04933336
反応ノート
読み込み中…