Sodium Hydroxide → Zinc Dodecyl Fumarate
反応式
[C:1]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])(=[O:7])/[CH:2]=[CH:3]/[C:4]([O-:6])=[O:5].[OH-].[Na+].O.O.C([O-])(=O)C.[Zn+2:29].C([O-])(=O)C>CC(C)=O>[C:1]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])(=[O:7])/[CH:2]=[CH:3]/[C:4]([O-:6])=[O:5].[Zn+2:29].[CH2:9]([O:8][C:1](=[O:7])/[CH:2]=[CH:3]/[C:4]([O-:6])=[O:5])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]参加物
5
反応条件
- 温度
- 50 °C
実験手順
To a 12 percent w/v acetone suspension of the monododecyl fumarate heated to 50° C. is added 1.0 molar equivalent sodium hydroxide (299 g) as a 10 percent w/v aqueous solution. After the stirred suspension clears, 0.5 molar equivalent zinc acetate dihydrate (110 g) as a saturated aqueous solution is added with stirring. The supernatant liquid is separated from the precipitated zinc dodecyl fumarate.