Ethyl 2-(phenylamino)-4-thiazolecarboxylate → HCID 15053553、化合物

HRID 2107260ノート

反応式

HRID 2107260 の反応式
[NH:1]([C:8]1[S:9][CH:10]=[C:11]([C:13](OCC)=[O:14])[N:12]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[NH:1]([C:8]1[S:9][CH:10]=[C:11]([CH2:13][OH:14])[N:12]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

参加物

4

反応物 2

HCID 15053537Ethyl 2-(phenylamino)-4-thiazolecarboxylateHCID 21226445Aluminium lithium hydride

生成物 1

HCID 15053553HCID 15053553、化合物

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

Following a procedure similar to that described in Preparation 15, the desired compound was prepared from 8.5 g of ethyl 2-anilinothiazol-4-carboxylate, 2 g of lithium aluminum hydride and 150 ml of tetrahydrofuran, as colorless flakes having the following physical properties.

後処理

  1. customthat described in Preparation 15

出典と根拠

ORDレコード
ord-709e174847f74fbd8903fb05c07ba5d1
出典データセット
uspto-grants-1990_06
特許番号
US04933355

反応ノート

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