化工社化工社 化学情報印刷レポート · 研究参考用
3-(Methoxymethyl)benzeneboronic acid → 3-(3'-Methoxymethyl-biphenyl-4-yloxymethyl)-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Methoxymethyl)benzeneboronic acid | HCID 3825855 | — |
| 反応物 | Methyl 3-((4-iodophenoxy)methyl)benzoate | HCID 57643351 | — |
| 生成物 | 3-(3'-Methoxymethyl-biphenyl-4-yloxymethyl)-benzoic acid | HCID 11581062 | — |
反応手順
3-(3′-Methoxymethyl-biphenyl-4-yloxymethyl)-benzoic acid was prepared using the procedure described above for the preparation of Example 12 from 3-(4-iodo -phenoxymethyl)-benzoic acid methyl ester (of Intermediate 1) and 3-methoxymethylphenylboronic acid (available from Digital Specialty Chemicals, Inc., Dublin, N.H.). Mass spectrum MH+=349.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07524870B2 |
| 出典データセット | uspto-grants-2009_04 |
| ORD ID | ord-63867813441b41ef9a4c0340fb6e4768 |
| 出典メモ | uspto-grants-2009_04 |