4-(2,2-Dimethylpropyl)-2-(prop-2-en-1-yl)phenol → 4-(2,2-Dimethylpropyl)-2-propylphenol
反応式
[CH2:1]([C:4]1[CH:9]=[C:8]([CH2:10][C:11]([CH3:14])([CH3:13])[CH3:12])[CH:7]=[CH:6][C:5]=1[OH:15])[CH:2]=[CH2:3]>[Pd].C(OCC)(=O)C>[CH3:12][C:11]([CH3:13])([CH3:14])[CH2:10][C:8]1[CH:7]=[CH:6][C:5]([OH:15])=[C:4]([CH2:1][CH2:2][CH3:3])[CH:9]=1参加物
4
実験手順
A mixture of 2-allyl-4-(2,2-dimethyl-propyl)phenol (0.70 g, 3.4 mmol) and 10% palladium on carbon (0.14 g) in ethyl acetate was stirried under hydrogen (1 atm) for 1 h. The reaction mixture was filtered and the filtrate was concentrated to give the title compound.
後処理
- filtrationThe reaction mixture was filtered
- concentrationthe filtrate was concentrated
出典と根拠
- ORDレコード
- ord-7745f317d018492c91177168eab1c9e3
- 出典データセット
- uspto-grants-2009_04
- 特許番号
- US07524882B2
反応ノート
読み込み中…