Triethylamine → HCID 69245143、化合物
反応式
Cl[C:2]1[O:3][C:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[CH:5][N:6]=1.[F:13][C:14]([F:33])([F:32])[C:15]1[CH:16]=[C:17]([N:21]2[CH2:26][CH2:25][N:24]([CH2:27][CH2:28][CH2:29][CH2:30]N)[CH2:23][CH2:22]2)[CH:18]=[CH:19][CH:20]=1.C([N:36](CC)CC)C>O1CCCC1>[F:33][C:14]([F:13])([F:32])[C:15]1[CH:16]=[C:17]([N:21]2[CH2:22][CH2:23][N:24]([CH2:27][CH2:28][CH2:29][CH2:30][C:2]3[O:3][C:4]([C:7]4[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=4)=[C:5]([NH2:36])[N:6]=3)[CH2:25][CH2:26]2)[CH:18]=[CH:19][CH:20]=1参加物
5
実験手順
A solution of 35 mg (0.2 mmol) of 2-chloro-5-phenyloxazole in 0.5 mL of tetrahydrofuran is added, at 0° C., to a solution of 62 mg (0.2 mmol) of 4-[4-(3-trifluoromethylphenyl)piperazine-1-yl]butylamine (Example 3, step b) and 20 mg (0.2 mmol) of triethylamine in 0.2 mL of tetrahydrofuran. The mixture is stirred overnight under argon.