4-Vinylpyridine → HCID 22975755、化合物
反応式
Cl.NN=CC1C=CC([C:9]([N:11]2[CH2:16][CH2:15][C:14]3([CH2:21][CH2:20][CH:19]([CH2:22][C:23]([O:25][CH2:26][CH3:27])=[O:24])[CH2:18][CH2:17]3)[CH2:13][CH2:12]2)=O)=CC=1.[CH:30]([C:32]1[CH:37]=[CH:36][N:35]=[CH:34][CH:33]=1)=C>C(#N)C>[N:35]1[CH:36]=[CH:37][C:32]([CH2:30][CH2:9][N:11]2[CH2:16][CH2:15][C:14]3([CH2:21][CH2:20][CH:19]([CH2:22][C:23]([O:25][CH2:26][CH3:27])=[O:24])[CH2:18][CH2:17]3)[CH2:13][CH2:12]2)=[CH:33][CH:34]=1参加物
4
実験手順
A solution of 0.48 g (2.0 mmol) of the intermediate from Example 1. Step C and 0.21 g (2.0 mmol) 4-vinylpyridine in 6 ml acetonitrile were heated at 80° C. over night. The solvent was removed under reduced pressure, and the remaining solid title compound was purified by stirring several times with tert.-butylmethylether, filtered with suction, and dried in vacuo.
後処理
- customThe solvent was removed under reduced pressure