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Acetic Anhydride → Citronellyl Acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | Citronellol | HCID 8842 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | Citronellyl Acetate | HCID 9017 | — |
反応手順
100 Grams of 3,7-dimethyloct-6-en-1-ol is dissolved in 150 ml. of pyridine and 100 ml. of acetic anhydride and left at room temperature for about 48 hours. Then the mixture is extracted with ether and the ethereal extracts washed with water, 10% aqueous HCl and brine to yield 1-acetoxy-3,7-dimethyloct-6-ene which is purified by distillation.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04137273 |
| 出典データセット | uspto-grants-1979_01 |
| ORD ID | ord-bd39ca3e5fdc410baafd6f53f8e929f7 |
| 出典メモ | uspto-grants-1979_01 |