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HRID 2164189作成日:2026年10月27日

Acetic Anhydride → Citronellyl Acetate

https://huagongshe.com/reaction/2164189

反応式

関与物質

役割名称HCID仕込み量
反応物Acetic AnhydrideHCID 7918—
反応物CitronellolHCID 8842—
溶媒PyridineHCID 1049—
生成物Citronellyl AcetateHCID 9017—

反応手順

100 Grams of 3,7-dimethyloct-6-en-1-ol is dissolved in 150 ml. of pyridine and 100 ml. of acetic anhydride and left at room temperature for about 48 hours. Then the mixture is extracted with ether and the ethereal extracts washed with water, 10% aqueous HCl and brine to yield 1-acetoxy-3,7-dimethyloct-6-ene which is purified by distillation.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04137273
出典データセットuspto-grants-1979_01
ORD IDord-bd39ca3e5fdc410baafd6f53f8e929f7
出典メモuspto-grants-1979_01