3,5-Dimethyl-4-nitrocyclohex-1-ene → 2,6-Dimethylcyclohexylamine

HRID 2164687ノート

反応式

HRID 2164687 の反応式
[CH3:1][CH:2]1[CH:7]([N+:8]([O-])=O)[CH:6]([CH3:11])[CH2:5][CH:4]=[CH:3]1.[H][H]>[Pd]>[CH3:11][CH:6]1[CH2:5][CH2:4][CH2:3][CH:2]([CH3:1])[CH:7]1[NH2:8]

参加物

4

反応物 2

HCID 204053483,5-Dimethyl-4-nitrocyclohex-1-eneHCID 178418361HCID 178418361、化合物

生成物 1

HCID 1109322,6-Dimethylcyclohexylamine

試薬・触媒・溶媒 1

HCID 23938Palladium触媒

実験手順

contacting said 3,5-dimethyl-4-nitro-cyclohexene with hydrogen at a temperature of about 0° C. to about 200° C. and a pressure of about 0 psig to about 1500 psig in the presence of a palladium catalyst to form 2,6-dimethylcyclohexyl amine; and

後処理

  1. customat a temperature of about 0° C. to about 200° C.

出典と根拠

ORDレコード
ord-cdaada7ceb2a4cfe80bb83c656bd31ab
出典データセット
uspto-grants-1985_03
特許番号
US04506098

反応ノート

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