Benzoyl Peroxide → HCID 54546446、化合物
反応式
[CH3:1][C:2]([CH3:13])([CH3:12])[C:3]#[C:4][C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1.[Br:14]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1.CCCCCC>C(Cl)(Cl)(Cl)Cl>[CH3:1][C:2]([CH3:13])([CH3:12])[C:3]#[C:4][C:5]1[CH:6]=[CH:7][C:8]([CH2:11][Br:14])=[CH:9][CH:10]=1参加物
6
実験手順
3.35 g of 4-(3,3-Dimethyl-1-butynyl)toluene, 3.47 g of N-bromosuccinimide and 100 mg of dibenzoylperoxide in 50 ml of carbon tetrachloride are refluxed for 8 hours. The mixture is filtered and the solvent removed under vacuum. The pure product is obtained as an oil following chromatography over silica gel using hexane as an eluant.
後処理
- filtrationThe mixture is filtered
- customthe solvent removed under vacuum
- customThe pure product is obtained as an oil
出典と根拠
- ORDレコード
- ord-601813db736f4c16ade63c23595ec770
- 出典データセット
- uspto-grants-1990_07
- 特許番号
- US04939148
反応ノート
読み込み中…