Diethyl Ether → 3-Hydroxypropyl Dimethyl Nonyl Ammonium Iodide

HRID 2165350ノート

反応式

HRID 2165350 の反応式
[CH2:1]([I:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[CH3:11][N:12]([CH:14](O)[CH2:15][CH3:16])[CH3:13].CC[O:20]CC>C(#N)C>[I-:10].[OH:20][CH2:16][CH2:15][CH2:14][N+:12]([CH3:13])([CH3:11])[CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9]

参加物

5

反応物 3

HCID 3283Diethyl EtherHCID 202751-IodononaneHCID 116739Propanol, (dimethylamino)-

生成物 1

HCID 197748283-Hydroxypropyl Dimethyl Nonyl Ammonium Iodide収率 77%

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

Employing the procedure of EXAMPLE II, 20.0 g of nonyl iodide was reacted with 14.3 ml of N,N-dimethylaminopropanol in 50 ml of acetonitrile to provide a crude product which was slurried with ether to give 27 g (77%) of an amber oil which solidified on standing. Proton NMR confirmed the desired structure.

後処理

  1. customto provide a crude product which

出典と根拠

ORDレコード
ord-74ce965b426a4a7b8aef9f4b096ad4bb
出典データセット
uspto-grants-1990_07
特許番号
US04939289

反応ノート

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