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Aniline → allyl N-phenyl-2,3-epoxysuccinamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | HCID 178455845 | HCID 178455845 | — |
| 生成物 | allyl N-phenyl-2,3-epoxysuccinamate | HCID 13150874 | 50.7% |
反応手順
Following the procedure of Example 1, monoallyl potassium epoxysuccinate (2.1 g) was successively treated with oxalyl chloride (1.26 g) and aniline (1.86 g) to give 1.24 g of allyl N-phenyl-2,3-epoxysuccinamate (Compound No. 30) as colorless needles melting at 32° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04387238 |
| 出典データセット | uspto-grants-1983_06 |
| ORD ID | ord-e3b567c51b564631b0ab7bafbf747871 |
| 出典メモ | uspto-grants-1983_06 |