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HRID 2166957作成日:2026年10月27日

Ethanol → 4-p-Tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid

https://huagongshe.com/reaction/2166957

反応式

関与物質

役割名称HCID仕込み量
反応物EthanolHCID 702—
反応物Sodium HydroxideHCID 14798—
反応物Methyl 4-p-tolylsulfonyl-4-methyl-3-dimethoxymethylpentanoateHCID 12850320—
溶媒WaterHCID 962—
生成物4-p-Tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acidHCID 12850317—

反応手順

1 g of the product of Step A was added to a mixture of 20 ml of ethanol and 20 ml of aqueous 2 N sodium hydroxide solution and the mixture was refluxed for 17 hours and was cooled and poured into water. The mixture was extracted with methylene chloride and the organic phase was evaporated to dryness to obtain 4-p-tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04390724
出典データセットuspto-grants-1983_06
ORD IDord-1f8589769f9842c4948589fc9c8644e6
出典メモuspto-grants-1983_06