化工社化工社 化学情報印刷レポート · 研究参考用
Ethanol → 4-p-Tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Methyl 4-p-tolylsulfonyl-4-methyl-3-dimethoxymethylpentanoate | HCID 12850320 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-p-Tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid | HCID 12850317 | — |
反応手順
1 g of the product of Step A was added to a mixture of 20 ml of ethanol and 20 ml of aqueous 2 N sodium hydroxide solution and the mixture was refluxed for 17 hours and was cooled and poured into water. The mixture was extracted with methylene chloride and the organic phase was evaporated to dryness to obtain 4-p-tolylsulfonyl-4-methyl-3-dimethoxymethyl-pentanoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04390724 |
| 出典データセット | uspto-grants-1983_06 |
| ORD ID | ord-1f8589769f9842c4948589fc9c8644e6 |
| 出典メモ | uspto-grants-1983_06 |