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HRID 2175260作成日：2026年10月27日

tert-Butyl 3-(bromomethyl)phenylcarbamate → 1-(5-(1-(1-(3-Aminophenyl)ethyl)-1H-pyrazol-4-yl)-3,4-dihydroquinolin-1(2H)-yl)-4-(2,3-dimethylphenoxy)butan-1-one

https://huagongshe.com/reaction/2175260

反応式

関与物質

役割名称HCID仕込み量
反応物tert-Butyl 3-(bromomethyl)phenylcarbamateHCID 14523558—
反応物1-(5-(1-(3-Aminobenzyl)-1H-pyrazol-4-yl)-3,4-dihydroquinolin-1(2H)-yl)-4-(2,3-dimethylphenoxy)butan-1-oneHCID 86712585—
反応物tert-Butyl 3-(1-bromoethyl)phenylcarbamateHCID 86712586—
生成物1-(5-(1-(1-(3-Aminophenyl)ethyl)-1H-pyrazol-4-yl)-3,4-dihydroquinolin-1(2H)-yl)-4-(2,3-dimethylphenoxy)butan-1-oneHCID 86712587—

反応手順

The title compound was prepared using a procedure analogous to 1-(5-(1-(3-aminobenzyl)-1H-pyrazol-4-yl)-3,4-dihydroquinolin-1(2H)-yl)-4-(2,3-dimethylphenoxy)butan-1-one except that tert-butyl 3-(bromomethyl)phenylcarbamate was replaced with tert-butyl 3-(1-bromoethyl)phenylcarbamate. LCMS, [M+H]+=509.5.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09062028B2
出典データセットuspto-grants-2015_06
ORD IDord-6de6a5d602fa405388305c873c898a3a
出典メモuspto-grants-2015_06