Ethyl 2-(3-vinylphenyl)acetate → Ethyl 2-(3-ethylphenyl)acetate
反応式
[CH:1]([C:3]1[CH:4]=[C:5]([CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:6]=[CH:7][CH:8]=1)=[CH2:2]>C(O)C.[Pd]>[CH2:1]([C:3]1[CH:4]=[C:5]([CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:6]=[CH:7][CH:8]=1)[CH3:2]参加物
4
反応条件
- 温度
- 30 °C
実験手順
To a solution of ethyl 2-(3-vinylphenyl)acetate (640 mg, 3.6 mmol) in ethanol (10 mL) was added 10% of Pd/C (100 mg) and stirred at 30° C. under hydrogen atmosphere (15 psi) for 7 hours. Then the solution was filtered and the solvent was removed in vacuo (500 mg, yield 77%).
後処理
- filtrationThen the solution was filtered
- customthe solvent was removed in vacuo (500 mg, yield 77%)
出典と根拠
- ORDレコード
- ord-6005ba9a255d4059ac2b01de347e9246
- 出典データセット
- uspto-grants-2015_06
- 特許番号
- US09067893B2
反応ノート
読み込み中…