Hydrazine → N-(3-Aminopropyl)morpholine

HRID 21785

反応式

HRID 21785 の反応式
[NH2:1]N.[N:3]1([CH2:9][CH2:10][CH2:11]C2C=CC=C3C(NC(=O)C=23)=O)[CH2:8][CH2:7][O:6][CH2:5][CH2:4]1>CO>[N:3]1([CH2:9][CH2:10][CH2:11][NH2:1])[CH2:4][CH2:5][O:6][CH2:7][CH2:8]1

参加物

4

反応物 2

HCID 9321HydrazineHCID 1317183813-Morpholinylpropylphthalimide

生成物 1

HCID 61055N-(3-Aminopropyl)morpholine

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 3-morpholinylpropylphthalimide (219 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

後処理

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

出典と根拠

ORDレコード
ord-31cf6c6cd592407aaa6aa050e8dff730
出典データセット
uspto-grants-1995_06
特許番号
US05424451

関連ノート

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