Sodium Hydroxide → 4-(3,4-Dimethoxybenzoyl)benzoic acid

HRID 2187957ノート

反応式

HRID 2187957 の反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[C:6]([C:8]1[CH:17]=[CH:16][C:11]([C:12]([O:14]C)=[O:13])=[CH:10][CH:9]=1)=[O:7].[OH-].[Na+]>C(O)C>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:18]=[CH:19][C:20]=1[O:21][CH3:22])[C:6]([C:8]1[CH:17]=[CH:16][C:11]([C:12]([OH:14])=[O:13])=[CH:10][CH:9]=1)=[O:7]

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 22645197Methyl 4-(3,4-dimethoxybenzoyl)benzoate

生成物 1

HCID 226452014-(3,4-Dimethoxybenzoyl)benzoic acid

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

1.3 g (4.33 mmol) of methyl 4-(3,4-dimethoxybenzoyl)benzoate was dissolved in 50 ml of ethanol. 7 ml of 1 N sodium hydroxide solution was added to the obtained solution, and they were stirred overnight. The solvent was evaporated, and the residue was washed with ethyl acetate and then filtered to obtain the title compound.

後処理

  1. customThe solvent was evaporated
  2. washthe residue was washed with ethyl acetate
  3. filtrationfiltered

出典と根拠

ORDレコード
ord-098d053346434bc58ad69083a0b2469d
出典データセット
uspto-grants-2002_06
特許番号
US06410538B2

反応ノート

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