Ammonia → HCID 131727632、化合物

反応式

[C:1]([C:5]([C:8]([C:11]([O:14][CH2:15][C:16]([C:19]([OH:21])=[O:20])([F:18])[F:17])([F:13])[F:12])([F:10])[F:9])([F:7])[F:6])([F:4])([F:3])[F:2].[NH3:22].[OH-].[Na+]>>[C:1]([C:5]([C:8]([C:11]([O:14][CH2:15][C:16]([C:19]([O-:21])=[O:20])([F:18])[F:17])([F:12])[F:13])([F:10])[F:9])([F:7])[F:6])([F:4])([F:3])[F:2].[NH4+:22]

参加物

反応物 3

HCID 222Ammonia

HCID 14798Sodium Hydroxide

HCID 714186542,2-Difluoro-3-(nonafluorobutoxy)propanoic acid

生成物 1

HCID 131727632HCID 131727632、化合物

実験手順

An aqueous solution of CF3CF2CF2CF2OCH2CF2COONH4 was prepared in the same manner as in Synthesis Example 1 except that the CF3CF2CF2CF2OCH2CF2COOH prepared in Synthesis Example 3 was neutralized to pH 7 using aqueous ammonia in lieu of the aqueous solution of sodium hydroxide.