Iodoethane → 4-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1-ethyl-1H-pyridin-2-one

反応式

[CH3:1][C:2]1[N:3]([C:17]2[CH:22]=[CH:21][NH:20][C:19](=[O:23])[CH:18]=2)[C:4]([CH3:16])=[C:5]([C:7]#[C:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)[N:6]=1.[CH2:24](I)[CH3:25]>>[CH3:1][C:2]1[N:3]([C:17]2[CH:22]=[CH:21][N:20]([CH2:24][CH3:25])[C:19](=[O:23])[CH:18]=2)[C:4]([CH3:16])=[C:5]([C:7]#[C:8][C:9]2[CH:10]=[C:11]([CH3:15])[CH:12]=[CH:13][CH:14]=2)[N:6]=1

参加物

反応物 2

HCID 6340Iodoethane

HCID 581111894-(2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl)-1H-pyridin-2-one

生成物 1

HCID 498727654-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1-ethyl-1H-pyridin-2-one

実験手順

The title compound, light brown solid, MS: m/e=332.2 (M+H+), was prepared in accordance with the general method of example 3 from 4-[2,5-dimethyl-4-m-tolylethynyl-imidazol-1-yl]-1H-pyridin-2-one and ethyl iodide.

出典と根拠

ORDレコード: ord-2b578f28f6474663baa0f301d47aff2e
出典データセット: uspto-grants-2012_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08334287B2

反応ノート

読み込み中…