Salicyl Alcohol → 2-[(Ethylsulfanyl)methyl]phenol
反応式
O[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9].[CH2:10]([SH:12])[CH3:11]>>[CH2:10]([S:12][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9])[CH3:11]参加物
3
実験手順
A mixture of 49.6 g (0.4 mol) of 2-hydroxymethyl-phenol and 124 g (2 mol) of ethylmercaptan was heated for 5 hours to 170° C. in a stirred autoclave. Working up as in Example 1 gave 32.2 g (96% of theory) of 2-ethylthiomethyl-phenol.
後処理
- temperaturewas heated for 5 hours to 170° C. in a stirred autoclave
出典と根拠
- ORDレコード
- ord-eacb17e009e84059b307f1326fc1641a
- 出典データセット
- uspto-grants-1982_11
- 特許番号
- US04358616
反応ノート
読み込み中…