2-Bromopropane → HCID 20519071、化合物

HRID 2198798

反応式

HRID 2198798 の反応式
[OH:1][CH2:2][CH:3]1[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.Br[CH:16]([CH3:18])[CH3:17]>O>[CH:3]1([CH2:2][O:1][CH:16]([CH3:18])[CH3:17])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]1

参加物

4

反応物 2

HCID 63582-BromopropaneHCID 74686Cyclododecanemethanol

生成物 1

HCID 20519071HCID 20519071、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

According to the disclosure of Example 1, 99 g of hydroxymethylcyclododecane was first converted into the sodium alcoholate. 74 g (0.6 mol) of 2-bromopropane was added dropwise to the boiling suspension, and then the mixture was heated for 30 hours under reflux. The reaction mixture was poured into water, the organic phase was washed with water, dried over Na2SO4, and then distilled.

後処理

  1. temperaturethe mixture was heated for 30 hours
  2. temperatureunder reflux
  3. washthe organic phase was washed with water
  4. dry with materialdried over Na2SO4
  5. distillationdistilled

出典と根拠

ORDレコード
ord-dcbf17b5baba4e33805706cfee481f0a
出典データセット
uspto-grants-1982_11
特許番号
US04359588

関連ノート

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