Glycerol → 2-Propenoic acid, 3-phenyl-
反応式
CO[C:3]1[CH:17]=[CH:16][CH:15]=[CH:14][C:4]=1[C:5](OC)=[C:6](OC)[C:7]([OH:9])=[O:8].C1OC1CO.S(=O)(=O)(O)O.OCC(CO)O>CS(C)=O>[C:7]([OH:9])(=[O:8])[CH:6]=[CH:5][C:4]1[CH:3]=[CH:17][CH:16]=[CH:15][CH:14]=1参加物
6
反応条件
- 温度
- 90 °C
実験手順
4.35 g of trimethoxy cinnamic acid and 10 g of glycidol were dissolved in 5 ml of DMSO. The mixture was stirred and heated to 90° C. Catalystic amount of sulfuric acid was added, heating and agitation were carried out for 3.5 hours, and then the adduct of cinnamic acid and glycerin was obtained.
後処理
- temperatureheating
出典と根拠
- ORDレコード
- ord-ff8a7db881944361986decaa997cade8
- 出典データセット
- uspto-grants-1995_06
- 特許番号
- US05426210
反応ノート
読み込み中…