Thionyl Chloride → HCID 88422751、化合物

反応式

[CH3:1][C:2]1[CH:3]=[C:4]([CH:11]=[C:12]([CH3:14])[CH:13]=1)[CH2:5][CH:6]([OH:10])[C:7](O)=[O:8].S(Cl)([Cl:17])=O>>[CH3:1][C:2]1[CH:3]=[C:4]([CH:11]=[C:12]([CH3:14])[CH:13]=1)[CH2:5][CH:6]([OH:10])[C:7]([Cl:17])=[O:8]

参加物

反応物 2

HCID 24386Thionyl Chloride

HCID 19379351HCID 19379351、化合物

生成物 1

HCID 88422751HCID 88422751、化合物

実験手順

3,5-Dimethyl benzyl glycolic acid (5.59 g) was cooled to 0° C. Thionyl chloride (5 ml) was added and the stirred solution was refluxed for 2 h. The solvent was removed in vacuo to afford 3,5-dimethyl benzyl glycolic acid chloride as an oil.

後処理

temperaturethe stirred solution was refluxed for 2 h
customThe solvent was removed in vacuo

出典と根拠

ORDレコード: ord-dd92091af385400ca76de8145c5d9c4b
出典データセット: uspto-grants-1995_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05459270

反応ノート

読み込み中…

参加物