Hydrochloric Acid → HCID 17978210、化合物
反応式
[CH3:1][N:2]([CH:4]([CH3:6])C)[CH3:3].[ClH:7].[CH3:8][CH2:9][CH2:10][CH2:11][CH2:12]CC>>[ClH:7].[CH3:1][NH+:2]([CH2:4][C:6]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH3:3]参加物
4
実験手順
6 g of N,N-dimethylisopropylamine and 300 ml of heptane were placed under argon in a 500 ml three-necked flask fitted with internal thermometer and gas inlet stopcock. HCl gas from a gas generation apparatus was passed into this reaction mixture for 1 hour. The N,N-dimethylbenzylammonium hydrochloride formed was separated off via a G4 frit, washed with 100 ml of heptane and dried in an oil pump vacuum. 7.4 g (87%) of the desired product were isolated.
後処理
- customfitted with internal thermometer and gas inlet stopcock
出典と根拠
- ORDレコード
- ord-01a518d5a7e9418f8b86a78642d989fa
- 出典データセット
- uspto-grants-2006_09
- 特許番号
- US07101940B2
反応ノート
読み込み中…