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llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
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Oxygen → Silica

HRID 22152
ノート
印刷プレビュー

反応式

HRID 22152 の反応式
O=O.[Si:3]([OH:7])([OH:6])([OH:5])[OH:4].[OH-].[Na+:9]>>[Si:3]([O-:7])([O-:6])([O-:5])[O-:4].[Na+:9].[Na+:9].[Na+:9].[Na+:9].[Si:3](=[O:5])=[O:4]
参加物実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 977OxygenHCID 14798Sodium HydroxideHCID 14942Orthosilicic acid

生成物 2

HCID 24261SilicaHCID 26051Sodium orthosilicate

実験手順

Oxygen cleaning agent according to the invention was made as follows: a highly concentrated sodium silicate solution was prepared by reacting 45.4 kilograms of 99.9% silicic acid with 93.0 kilograms of 50% sodium hydroxide solution at 104.4° C. to 126.7° C. This temperature was maintained for four hours under reflux conditions not allowing the temperature to exceed 126.7° C. This material was then quenched with 68.0 kilograms of ASTM D1193 Type 1 demineralized water. Two hundred and twenty five grams of this 44% active polysilicate anion sodium silicate solution was mixed with one liter of ASTM D1193 Type 1 demineralized water to obtain a silicon dioxide:disodium oxide mole ratio of 1.83, a polysilicate anion concentration of 9.5% by weight and a pH of 12.4. This solution was then heated to 82.2° C. for two hours and filtered in steps through 50 micron, 10 micron and 3 micron filters. The solution was allowed to cool to room temperature, and five grams of 99.9% sodium molybdate was added as a corrosion inhibitor. Then 15 grams of 48 to 50% fluoroboric acid was added as an additional corrosion inhibitor reducing the pH to 11.93 and forming in situ sodium fluoroborate.

後処理

  1. customat 104.4° C. to 126.7° C
  2. temperatureThis temperature was maintained for four hours under reflux conditions not
  3. customto exceed 126.7° C
  4. customThis material was then quenched with 68.0 kilograms of ASTM D1193 Type 1 demineralized water
  5. additionTwo hundred and twenty five grams of this 44% active polysilicate anion sodium silicate solution was mixed with one liter of ASTM D1193 Type 1 demineralized water

出典と根拠

ORDレコード
ord-8847c530e1c54cc3bf0dabe2acfb6bf3
出典データセット
uspto-grants-1995_06
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US05427709

反応ノート

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