関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrogen Bromide | HCID 260 | — |
| 反応物 | 2-Benzyl-6-methoxypyridine | HCID 21942274 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178515992 | HCID 178515992 | 70.9% |
反応手順
A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07112593B2 |
|---|
| 出典データセット | uspto-grants-2006_09 |
|---|
| ORD ID | ord-8432c46a7bbf42feb057a7de3b73cea2 |
|---|
| 出典メモ | uspto-grants-2006_09 |
|---|
