Ethanol → L-Isoleucine
反応式
[OH-].[Na+].[NH3:3].[C:4]([OH:11])(=[O:10])/[CH:5]=[CH:6]/[C:7](O)=O.[CH2:12](O)[CH3:13]>>[NH2:3][C@H:5]([C:4]([OH:11])=[O:10])[C@H:6]([CH2:12][CH3:13])[CH3:7]参加物
4
実験手順
On a pilot-plant scale the free amine is prepared by the addition of NaOH/NH3. Fumaric acid is dissolved in hot ethanol, the free amine is added dropwise, and (Ile-Thia)2 furmarate (M=520.71 gmol−1) precipitates. The analysis of isomers and enantiomers is carried out by electrophoresis.
後処理
- custom(Ile-Thia)2 furmarate (M=520.71 gmol−1) precipitates
出典と根拠
- ORDレコード
- ord-35b54e5b223c420db535d8d0f81e9fda
- 出典データセット
- uspto-grants-2008_05
- 特許番号
- US07368421B2
反応ノート
読み込み中…