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4-Chlorophenol → 1-(4-Chlorophenoxy)acetone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorophenol | HCID 4684 | — |
| 反応物 | Chloroacetone | HCID 6571 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 1-(4-Chlorophenoxy)acetone | HCID 239874 | — |
反応手順
A suspension of 4-chlorophenol (2.6 g, 20 mmol), chloroacetone (2.8 g, 30 mmol) and potassium carbonate (3.45 g, 25 mmol) in acetone (100 ml) is heated at reflux for 3 hours. The precipitating inorganic salts are filtered off and the filtrate is evaporated to dryness to give the 1-(4-chlorophenoxy)-propan-2-one.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07368479B2 |
| 出典データセット | uspto-grants-2008_05 |
| ORD ID | ord-65a19d1a749045648c581d1c864878ce |
| 出典メモ | uspto-grants-2008_05 |