Oxalyl chloride → (4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)acetyl chloride
反応式
[CH3:1][C:2]([CH3:16])=[CH:3][CH2:4][CH2:5][C:6]1[CH2:11][CH2:10][CH:9]([CH2:12][C:13](O)=[O:14])[CH2:8][CH:7]=1.C(Cl)(=O)C([Cl:20])=O>>[CH3:1][C:2]([CH3:16])=[CH:3][CH2:4][CH2:5][C:6]1[CH2:11][CH2:10][CH:9]([CH2:12][C:13]([Cl:20])=[O:14])[CH2:8][CH:7]=1参加物
3
実験手順
To a 100 mL flask containing a stirbar is added the acid 2B (R=4-Methyl-3-pentenyl) (10 g) and oxalyl chloride (8.3 mL). The reaction is stirred under a nitrogen atmosphere for one hour after gas evolution ceases. Residual oxalyl chloride is removed in vacuo.
後処理
- additionTo a 100 mL flask containing a stirbar
- customResidual oxalyl chloride is removed in vacuo
出典と根拠
- ORDレコード
- ord-f7a2900f3ceb4afbb7ca027c24dcc3cd
- 出典データセット
- uspto-grants-2002_07
- 特許番号
- US06413448B1
反応ノート
読み込み中…