Hydroxyamine hydrochloride → 4-Ethyl2-hydroxyimino-5-nitro-hexanamide

反応式

[CH2:1]([CH:3]([CH:10]([N+:12]([O-:14])=[O:13])[CH3:11])[CH2:4][C:5](=O)[C:6]([NH2:8])=[O:7])[CH3:2].Cl.[NH2:16][OH:17]>>[CH2:1]([CH:3]([CH:10]([N+:12]([O-:14])=[O:13])[CH3:11])[CH2:4][C:5](=[N:16][OH:17])[C:6]([NH2:8])=[O:7])[CH3:2]

参加物

反応物 2

HCID 443297Hydroxyamine hydrochloride

HCID 14329816HCID 14329816、化合物

生成物 1

HCID 867424064-Ethyl2-hydroxyimino-5-nitro-hexanamide収率 69.8%

実験手順

4-Ethyl-2-hydroxyimino-5-nitro-hexanamide (15 mg) was prepared in the substantially same manner as that of Example 24 from 4-ethyl-5-nitro-2-oxo-hexanamide (20 mg) and hydroxylamine hydrochloride (14 mg).

出典と根拠

ORDレコード: ord-cbc8ebecda664d3ba4c8d306af639ad1
出典データセット: uspto-grants-1988_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04782088

反応ノート

読み込み中…