Iodoethane → 1-(3-Chloro-5-trifluoromethyl-phenyl)-4-ethyl-piperazine

HRID 2232895ノート

反応式

HRID 2232895 の反応式
[Cl:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.I[CH2:19][CH3:20]>>[Cl:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][N:15]([CH2:19][CH3:20])[CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:7]=1

参加物

3

反応物 2

HCID 6340IodoethaneHCID 223451951-(3-Chloro-5-(trifluoromethyl)phenyl)piperazine

生成物 1

HCID 223452151-(3-Chloro-5-trifluoromethyl-phenyl)-4-ethyl-piperazine

実験手順

Beginning with 1-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine and iodoethane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV)) 292 (M+, bp), 277 (88), 234 (33), 206 (55), 179 (49).

後処理

  1. customthe title compound was recovered by the procedure

出典と根拠

ORDレコード
ord-a7d4e2464276428ba533abc94137ea18
出典データセット
uspto-grants-2010_05
特許番号
USRE041315E1

反応ノート

読み込み中…