Allyl bromide → 1-Allyl-4-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine

HRID 2232927ノート

反応式

HRID 2232927 の反応式
[Cl:1][C:2]1[CH:3]=[C:4]([N:12]2[CH2:17][CH2:16][NH:15][CH2:14][CH2:13]2)[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[CH2:18](Br)[CH:19]=[CH2:20]>>[CH2:20]([N:15]1[CH2:16][CH2:17][N:12]([C:4]2[CH:5]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:7]=[C:2]([Cl:1])[CH:3]=2)[CH2:13][CH2:14]1)[CH:19]=[CH2:18]

参加物

3

反応物 2

HCID 7841Allyl bromideHCID 223451951-(3-Chloro-5-(trifluoromethyl)phenyl)piperazine

生成物 1

HCID 223451741-Allyl-4-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine

実験手順

Beginning with 1-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine and allylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV)) 305 (M+, 7), 96 (57), 69 (bp), 68 (48), 56 (69).

後処理

  1. customthe title compound was recovered by the procedure

出典と根拠

ORDレコード
ord-3c38614e047e4282b46fca1c66441759
出典データセット
uspto-grants-2010_05
特許番号
USRE041315E1

反応ノート

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