Ethyl p-methylbenzenesulfonate → 3-Ethyl-2-(ethylsulfanyl)-1,3-benzothiazol-3-ium 4-methylbenzene-1-sulfonate

HRID 223755

反応式

HRID 223755 の反応式
S[C:2]1[S:3][C:4]2[CH:10]=CC=[CH:7][C:5]=2[N:6]=1.[C:11]1([CH3:23])[CH:16]=[CH:15][C:14]([S:17]([O:20]CC)(=[O:19])=[O:18])=[CH:13][CH:12]=1>C(O)C>[C:11]1([CH3:23])[CH:12]=[CH:13][C:14]([S:17]([O-:20])(=[O:18])=[O:19])=[CH:15][CH:16]=1.[CH2:4]([S:3][C:2]1[S:17][C:14]2[CH:13]=[CH:12][CH:11]=[CH:16][C:15]=2[N+:6]=1[CH2:5][CH3:7])[CH3:10]

参加物

4

反応物 2

HCID 6638Ethyl p-methylbenzenesulfonateHCID 178418395HCID 178418395、化合物

生成物 1

HCID 140905473-Ethyl-2-(ethylsulfanyl)-1,3-benzothiazol-3-ium 4-methylbenzene-1-sulfonate

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒2 回

反応条件

温度
150 °C

実験手順

A mixture of 3.3 g of 2-mercaptobenzothiazole and 10.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C. and then 30 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzothiazolium p-toluenesulfonate.

後処理

  1. customto react them for 6 hours
  2. temperatureThe reaction product was cooled to 80° C.

出典と根拠

ORDレコード
ord-fab06d8802f34d2882e5fc578177755c
出典データセット
uspto-grants-1982_10
特許番号
US04356247

関連ノート

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