関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,2-Epoxydodecane | HCID 17858 | — |
| 反応物 | 2-(1H-imidazol-2-yl)pyridine | HCID 589313 | — |
| 触媒 | Water | HCID 962 | — |
| 生成物 | 1-(2-Hydroxydodecyl)-2-(2-pyridyl)imidazole | HCID 20520762 | — |
反応手順
A mixture of 14.5 g (0.1 mole) 2-(2-pyridyl)imidazole, 18.4 g (0.1 mole) 1,2-epoxydodecane and 3 drops of water was heated with stirring at about 160° C. under nitrogen for about one hour. The resulting product was then extracted with hot hexane and collected as yellow crystals which had a melting point of 62°-65° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04356309 |
|---|
| 出典データセット | uspto-grants-1982_10 |
|---|
| ORD ID | ord-a370c73d7c074116a7ccd29da8475232 |
|---|
| 出典メモ | uspto-grants-1982_10 |
|---|
