HRID223772

反应详情

EQUATION

反应方程式

HRID 223772 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
160 °C

PROCEDURE

实验过程

A mixture of 14.5 g (0.1 mole) 2-(2-pyridyl)imidazole, 18.4 g (0.1 mole) 1,2-epoxydodecane and 3 drops of water was heated with stirring at about 160° C. under nitrogen for about one hour. The resulting product was then extracted with hot hexane and collected as yellow crystals which had a melting point of 62°-65° C.

WORKUP

后处理

  1. temperaturewas heated
  2. extractionThe resulting product was then extracted with hot hexane
  3. customcollected as yellow crystals which