化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 4-Oxo-2-adamantyl chloromethyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | 4-Hydroxyadamantan-2-one | HCID 533435 | — |
| 生成物 | 4-Oxo-2-adamantyl chloromethyl ether | HCID 23150860 | — |
反応手順
Paraformaldehyde was added to 4-oxo-2-hydroxyadamantane, and a hydrogen chloride gas was injected at 2.5 equivalent amounts per this 4-oxo-2-hydroxyadamantane. Then, the reaction was conducted at a temperature of 50° C. for 12 hours. After the completion of the reaction, the product was distillated under reduced pressure so as to obtain 4-oxo-2-adamantyl chloromethyl ether (compound 1) represented by the following chemical formula (58).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07723007B2 |
| 出典データセット | uspto-grants-2010_05 |
| ORD ID | ord-de9da7268278471faa1a361f851be596 |
| 出典メモ | uspto-grants-2010_05 |