Sodium hydride → HCID 14988300、化合物

反応式

[N:1]1[CH:6]=[CH:5][C:4]([NH:7][N:8]2[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[CH:10]=[CH:9]2)=[CH:3][CH:2]=1.[CH3:17][N:18]([CH2:20][CH2:21][CH2:22]Cl)[CH3:19].[H-].[Na+]>>[CH3:17][N:18]([CH2:20][CH2:21][CH2:22][N:7]([C:4]1[CH:3]=[CH:2][N:1]=[CH:6][CH:5]=1)[N:8]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:10]=[CH:9]1)[CH3:19]

参加物

反応物 3

HCID 24758Sodium hydride

HCID 669603-Chloro-N,N-dimethyl-1-propanamine

HCID 3081186N-(4-pyridinyl)-1H-indol-1-amine

生成物 1

HCID 14988300HCID 14988300、化合物

実験手順

The title compound was prepared from N-(4-pyridinyl)-1H-indol-1-amine and dimethylaminopropyl chloride with the aid of NaH in substantially the same manner as in Example 4. The product was obtained as an oil.

後処理

customThe product was obtained as an oil

出典と根拠

ORDレコード: ord-02130e6a1b6f49018d5139ca0460a005
出典データセット: uspto-grants-1991_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05039811

反応ノート

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