M-Cresol → Cresentyl

HRID 2248529ノート

反応式

HRID 2248529 の反応式
[CH:1]1[C:6]([OH:7])=[CH:5][CH:4]=[CH:3][C:2]=1[CH3:8].[C:9](Cl)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>[OH-].[Na+]>[C:9]([O:7][C:6]1[CH:5]=[CH:4][CH:3]=[C:2]([CH3:8])[CH:1]=1)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

参加物

4

反応物 2

HCID 342M-CresolHCID 7412Benzoyl chloride

生成物 1

HCID 69193Cresentyl

試薬・触媒・溶媒 1

HCID 14798Sodium Hydroxide溶媒

実験手順

Metacresyl benzoate was prepared by vigorously shaking a mixture of metacresol (1 equivalent, 5 grams) and benzoyl chloride (1.2 equivalents, 7.1 grams) in a 10% aqueous solution of sodium hydroxide (100 ml) in a stoppered flask for 15 minutes. The white crystalline solid thus formed was removed by filtration, washed with water and dried to yield metacresyl benzoate.

後処理

  1. customMetacresyl benzoate was prepared
  2. customThe white crystalline solid thus formed
  3. customwas removed by filtration
  4. washwashed with water
  5. customdried

出典と根拠

ORDレコード
ord-ba7d5364089d403682484ba65b5e582d
出典データセット
uspto-grants-1991_08
特許番号
US05041169

反応ノート

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