4-Chlorotoluene → Tris(4-methylphenyl)sulfanium Chloride
反応式
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][CH:11]=2)=O)=[CH:4][CH:3]=1.[Cl:17][C:18]1[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=1>O>[Cl-:17].[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S+:8]([C:18]2[CH:23]=[CH:22][C:21]([CH3:24])=[CH:20][CH:19]=2)[C:10]2[CH:15]=[CH:14][C:13]([CH3:16])=[CH:12][CH:11]=2)=[CH:4][CH:3]=1参加物
4
実験手順
The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.
後処理
- customThe target compound was obtained
- customthe procedure of Synthesis Example 1 aside
- customin Synthesis Example 1
- extractionfor extraction
出典と根拠
- ORDレコード
- ord-7876b576d4b24804986972cc3496348e
- 出典データセット
- uspto-grants-2009_07
- 特許番号
- US07556909B2
反応ノート
読み込み中…