Isobutyric Acid → HCID 14870751、化合物

反応式

[CH3:1][N:2]1[CH:6]=[CH:5][CH:4]=[CH:3]1.[C:7](O)(=[O:11])[CH:8]([CH3:10])[CH3:9].N1C=CC=C1.C(O)(=O)CCCCCC>>[CH3:1][N:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[C:7](=[O:11])[CH:8]([CH3:10])[CH3:9]

参加物

反応物 4

HCID 6590Isobutyric Acid

HCID 73041-Methylpyrrole

HCID 8027Pyrrole

HCID 8094Heptanoic Acid

生成物 1

HCID 14870751HCID 14870751、化合物収率 80%

実験手順

Reaction and post-treatment were carried out in the same manner as in Example 12, except that 5.27 g (0.065 mole) of 1-methylpyrrole and 4.4 g (0.05 mole) of isobutyric acid were substituent for the pyrrole and heptanoic acid, to obtain 6 g of 1-methyl-2-isobutyrylpyrrole.

後処理

customReaction

出典と根拠

ORDレコード: ord-77ff4418637c43bc80e5a93ef8c0324c
出典データセット: uspto-grants-1993_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05235068

反応ノート

読み込み中…