Ethanimidic acid, ethyl ester, hydrochloride (1:1) → HCID 178439387、化合物

HRID 2260040ノート

反応式

HRID 2260040 の反応式
[NH2:1][C:2]1[CH:6]=[C:5]([CH2:7][CH2:8][CH3:9])[NH:4][N:3]=1.[ClH:10].[C:11](=[NH:16])(OCC)[CH3:12]>C(#N)C>[ClH:10].[CH2:7]([C:5]1[NH:4][N:3]=[C:2]([NH:1][C:11](=[NH:16])[CH3:12])[CH:6]=1)[CH2:8][CH3:9]

参加物

4

反応物 2

HCID 2724290Ethanimidic acid, ethyl ester, hydrochloride (1:1)HCID 222656845-Propyl-1H-pyrazol-3-amine

生成物 1

HCID 178439387HCID 178439387、化合物

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

A 11.5 g portion of 3-amino-5-propyl-1H-pyrazole was dissolved in 60 ml of acetonitrile, and 12.8 g of ethyl acetimidate hydrochloride was added to the above solution with cooling on an ice bath. The resulting mixture was stirred for 1 hour at the same temperature and then overnight at room temperature.

後処理

  1. temperaturewith cooling on an ice bath
  2. customovernight
  3. customat room temperature

出典と根拠

ORDレコード
ord-064c52bb5b48440fbb925e53e1ddedd9
出典データセット
uspto-grants-1995_12
特許番号
US05475114

反応ノート

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