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Potassium Hydroxide → N-(2,3-dihydroxypropyl)-N-dodecyl-2-hydroxyhexadecanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1,2-Propanediol, 3-(dodecylamino)- | HCID 102496 | — |
| 反応物 | Methyl 2-hydroxyhexadecanoate | HCID 543716 | — |
| 生成物 | N-(2,3-dihydroxypropyl)-N-dodecyl-2-hydroxyhexadecanamide | HCID 15825473 | — |
反応手順
N-(2,3-dihydroxypropyl)-N-dodecylamine (1.00 g, 0.0039 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum and methyl-2-hydroxyhexadecanoate (1.12 g, 0.0039 mole) was heated and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained (crude yield=1.9 g). The waxy solid was recrystalized from hot hexane (yield=1.26 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05476671 |
| 出典データセット | uspto-grants-1995_12 |
| ORD ID | ord-26d0ed40d8fa420097c96f1ceb2f5512 |
| 出典メモ | uspto-grants-1995_12 |