Thionyl Chloride → HCID 14674299、化合物
反応式
[C:1]([C:5]1[CH:9]=[C:8]([CH2:10]O)[O:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2].S(Cl)([Cl:14])=O>ClCCl>[C:1]([C:5]1[CH:9]=[C:8]([CH2:10][Cl:14])[O:7][N:6]=1)([CH3:4])([CH3:3])[CH3:2]参加物
4
実験手順
1.12 g of (3-t-butyl-isoxazol-5-yl)methanol was dissolved in 35 ml of dichloromethane, and 2.4 ml of thionyl chloride was added. The mixture was stirred at room temperature overnight. The reaction mixture was concentrated under reduced pressure. The residue was washed with hexane to obtain 1.12 g of 3-t-butyl-5-(chloromethyl)-isoxazole.
後処理
- concentrationThe reaction mixture was concentrated under reduced pressure
- washThe residue was washed with hexane
出典と根拠
- ORDレコード
- ord-356e4e5682644567a3388782d38711a5
- 出典データセット
- uspto-grants-2010_12
- 特許番号
- US07846956B2
反応ノート
読み込み中…