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Sodium Hydroxide → p-Trifluoromethoxybenzaldehyde oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | p-(Trifluoromethoxy)benzaldehyde | HCID 69573 | — |
| 反応物 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 生成物 | p-Trifluoromethoxybenzaldehyde oxime | HCID 2777199 | 94% |
反応手順
In a similar manner as described in Preparation Example 1, by using 4-(trifluoromethoxy)benzaldehyde (38.02 g, 200.0 mmol), sodium hydroxide (12.00 g, 300.0 mmol) and hydrochloric acid hydroxylamine (16.68 g, 240 mmol), a white solid required compound (38.68 g, 188 mmol, 94%) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09132126B2 |
| 出典データセット | uspto-grants-2015_09 |
| ORD ID | ord-2d1b21b657f145ceb454501707d3938c |
| 出典メモ | uspto-grants-2015_09 |