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HRID 2276621作成日:2026年10月25日

Bromobenzene → 1-Pentadecyl-3-phenoxybenzene

https://huagongshe.com/reaction/2276621

反応式

関与物質

役割名称HCID仕込み量
反応物BromobenzeneHCID 7961—
反応物DimethylacetamideHCID 31374—
反応物Hydrogenated cardanolHCID 68146—
反応物PotassiumHCID 5462222—
溶媒WaterHCID 962—
生成物1-Pentadecyl-3-phenoxybenzeneHCID 17747909—

反応条件

温度150 °C

反応手順

Into the round bottom flask containing potassium salt of 3-pentadecyl phenol is added bromobenzene followed by Cu powder and in a solvent, DMAc (dimethyl acetamide). The reaction mixture is heated at 150° C. for 6 h. After completion of the reaction, the obtained dark colored reaction mixture is poured into water and the Cu salts are removed by filtration. The filtrate is extracted in a solvent, washed with water and dried, purified to obtain arylated product, 1-pentadecyl-3-phenoxybenzene.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09133089B2
出典データセットuspto-grants-2015_09
ORD IDord-098d7520d0d44e888b6a85333b30fb9f
出典メモuspto-grants-2015_09