反应详情

温度

150 °C

Into the round bottom flask containing potassium salt of 3-pentadecyl phenol is added bromobenzene followed by Cu powder and in a solvent, DMAc (dimethyl acetamide). The reaction mixture is heated at 150° C. for 6 h. After completion of the reaction, the obtained dark colored reaction mixture is poured into water and the Cu salts are removed by filtration. The filtrate is extracted in a solvent, washed with water and dried, purified to obtain arylated product, 1-pentadecyl-3-phenoxybenzene.

1. customAfter completion of the reaction
2. customthe Cu salts are removed by filtration
3. extractionThe filtrate is extracted in a solvent
4. washwashed with water
5. customdried
6. custompurified