反応式
[NH2:1][C:2]1[CH:3]=[C:4]([NH:12][C:13]([NH:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)=[O:14])[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[C:23]([OH:31])(=[O:30])[C:24]([CH2:26][C:27](O)=[O:28])=[CH2:25]>>[O:28]=[C:27]1[N:1]([C:2]2[CH:7]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:5]=[C:4]([NH:12][C:13]([NH:15][CH2:16][C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[O:14])[CH:3]=2)[CH2:25][CH:24]([C:23]([OH:31])=[O:30])[CH2:26]1参加物
3
実験手順
A mixture of N-(3-amino-5-(trifluoromethyl)phenyl)(benzylamino)carboxamide and itaconic acid was fused at 110° C. for 10 hours. The resulted solid was washed with methanol and then dried at 50° C. for 12 hours.
後処理
- washThe resulted solid was washed with methanol
- customdried at 50° C. for 12 hours
出典と根拠
- ORDレコード
- ord-864cef6e6f664a059be8b4a512c33fb1
- 出典データセット
- uspto-grants-2005_02
- 特許番号
- US06849639B2
関連ノート
読み込み中…