HCID 20070371、化合物 → 1-Propanol, 2-[(2-aminophenyl)amino]-2-methyl-
反応式
[OH:1][CH2:2][C:3]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[N+:13]([O-])=O)([CH3:5])[CH3:4]>C(O)C.[Pd]>[OH:1][CH2:2][C:3]([NH:6][C:7]1[C:8]([NH2:13])=[CH:9][CH:10]=[CH:11][CH:12]=1)([CH3:5])[CH3:4]参加物
4
実験手順
N-(1-Hydroxy-2-methylprop-2-yl)-2-nitroaniline (10 g) in ethanol (200 ml) was hydrogenated over 5% palladium on charcoal (0.5 g) at 50 p.s.i. for 2 hours. The reaction was filtered and the solvent removed under vacuum to yield N-(1-hydroxy-2-methylprop-2-yl)benzene 1,2-diamine (8.4 g, 98%).
後処理
- filtrationThe reaction was filtered
- customthe solvent removed under vacuum
出典と根拠
- ORDレコード
- ord-3fbe53d520414a24ac3a540c5bbe68f0
- 出典データセット
- uspto-grants-1989_01
- 特許番号
- US04801598
反応ノート
読み込み中…